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▲ [6a-A204-4] Electrochemical reduction of diatom for the formation of silicon-film on silver-substrate
Keywords:diatom, electrochemical reduction, electrodeposition
Silicon (Si)-layer was formed on silver (Ag)-substrates using electrodeposition technique through electrochemical-reduction of purified (99%) diatomaceous earth (SiO2) in molten calcium chloride (CaCl2) at temperature of 855o C. Raman spectroscopy and X-ray diffraction (XRD) method confirm formation of poly-crystalline Si-film along with microcrystalline phases. Scanning electron microscopy (SEM) indicates Si-film has morphology with rough surfaces.